
Sampling Requirement
| Parameters |
Bottle Type | Sample Type | Preservative | Holding Time | Sampling Method |
| Ammonia as N [NH3N]* | Pint Plastic | Composite | H2SO4 to pH <2cool to 4° C | 28 days | EPA 350.1 |
| Arsenic | Pint Plastic | Composite | HNO3 to pH <2 coolto 4° C | 6 months | EPA 200.7 |
| BOD* | ½ Gal. Plastic | Composite | None cool to 4° C | 48 hours | SM 5210B |
| Cadmium | Pint Plastic | Composite | HNO3 to pH <2 cool to 4° C | 6 months | EPA 200.7 |
| Chromium | Pint Plastic | Composite | HNO3 to pH <2 cool to 4° C | 6 months | EPA 200.7 |
| Color (Purity & Luminance) |
Pint Plastic |
Grab | None cool to 4° C | 48 hours | SM 2120 |
| Copper | Pint Plastic | Composite | HNO3 to pH <2 cool to 4 ° C | 6 months | EPA 200.7 |
| Cyanide | Pint Plastic |
Grab | NaOH to pH >12 cool to 4° C | 14 days | SM 4500 |
| Lead | Pint Plastic | Composite | HNO3 to pH <2 cool to 4 ° C | 6 months | EPA 200.7 |
| Mercury | Pint Plastic |
Composite | HNO3 to pH <2 cool to 4 ° C | 6 months | EPA 600 245.1 |
| Molybdenum | Pint Plastic | Composite | HNO3 to pH <2 cool to 4 ° C | 6 months | EPA 200.7 |
| Nickel | Pint Plastic | Grab | HNO3 to pH <2 cool to 4 ° C | 6 months | EPA 200.7 |
| Total Oil & Grease |
Quart Glass |
Grab | H2SO4 to pH <2 cool to 4° C | 28 days | EPA 1664 HEM |
| Total Petroleum Hydrocarbons |
Quart Glass |
Grab |
HCl to pH <2 cool to 4° C | 28 days | EPA 1664 SGT |
| Phenols | 500 ml Amber Glass |
Grab | H2SO4 to pH <2 cool to 4° C | 28 days | EPA 420.2 |
| Selenium | Pint Plastic | Composite | HNO3 to pH <2 cool to 4° C | 6 months | EPA 200.7 |
| Silver | Pint Plastic |
Composite | HNO3 to pH <2 cool to 4° C | 6 months | EPA 200.7 |
| TSS* | Pint Plastic |
Composite | HNO3 to pH <2 cool to 4° C |
7days | SM 2540D |
| Zinc | Pint Plastic | Composite |
HNO3 to pH <2 cool to 4° C | 6 months | EPA 200.7 |
| Volatiles | 3 - 40ml VOA Vials | Grab | Zero headspace HCl to pH <2 cool to 4° C | 14 days | EPA 624 |
*Surchargeable Parameters
NOTES:
All sampling procedures must be in accordance with 40 CFR Part 136 and EAJSA Rules and Regulations.
Sample preservation must be performed immediately upon sample collection. Any self-monitoring conducted at the designated sample location (outlined in permit) which is in accordance with EPA approved procedure must be reported to the EAJSA (please note 1/28/00 memo). When using a different method for analysis you must notify the EAJSA prior.
References:
40 CFR Part 136
EPA’s Industrial User Inspection And Sampling Manual for POTWs (EPA 831-B-94-001).
Easton Area Joint Sewer Authority Rules and Regulations.

EAJSA
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